EFFECT OF COOLING-MEDIUM INDUCED INITIAL STRUCTURE BEFORE INTERCRITICAL ANNEALING ON THE MICROSTRUCTURE AND MECHANICAL PROPERTIES OF LOW ALLOY DUAL-PHASE STEEL

Toni Bambang Romijarso, Miftakhur Rohmah, Myrna Ariati, Efendi Mabruri, Eddy Sumarno Siradj

Abstract

The present research focused on determining the effect of cooling-medium-induced initial structure before the intercritical annealing induced dual-phase structure in the low alloy steel. Low carbon steel, which consists of containing 0.09 wt.% C was heated at 920 °C for 30 minutes to austenitization and then cooled in various media to provide the different initial structures before the IA (intercritical annealing) process. After austenization, the cooling process in the furnace and open-air provided a ferrite-pearlite phase, while the cooling process in water generated full martensite as the initial structure. Afterwards, the sample was intercritical-annealed at 750 °C (temperature between Ac1 and Ac3 lines or intercritical zone) for 10 minutes and then quenched in water. The water quenching after the austenitizing process improved the mechanical strength of steel (919 MPa), compared to the as-received state (519 MPa) due to martensite formation. As the cooling rate increased after the austenitizing process, the tensile strength increased and the elongation decreased. The different structures before intercritical annealing affected the martensite volume fraction and further correlated with improving mechanical properties. The ferrite and pearlite, as the initial structure before the IA process, provide a smaller fraction of martensite (18.36 vol.% for furnace cooling and 27.85 vol.% for open-air cooling). In contrast, the full martensite as the initial structure before IA generates a higher fraction of martensite (39.25 vol.%). The tensile strengths obtained were 512, 516, and 541 MPa with elongations of 29.8%, 30.1% and 32.6% for cooling furnace, open air and water, respectively. The strain-hardening behavior during the intercritical annealing is not affected by the initial process of the structure.

Keywords

Dual phase steel; intercritical anealing; low-alloy carbon steel; fraction of martensite

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References

M. Soliman and H. Palkowski, “Strain hardening dependence on the structure in dual-phase steels,” Steel Res. Int., vol. 92, no. 4, pp. 1-15, 2021. Doi: 10.1002/srin.202000518.

J. Samei, Y. Salib, M. Amirmaleki, and D. S. Wilkinson, “The role of microstructure on edge cracks in dual phase and quench and partitioning steels subject to severe cold rolling,” Scr. Mater., vol. 173, pp. 86-90, 2019. Doi: 10.1016/j.scriptamat.2019.08.012.

T. Yalçinkaya, S. O. Çakmak, and C. Tekoğlu, “A crystal plasticity based finite element framework for RVE calculations of two-phase materials: Void nucleation in dual-phase steels,” Finite Elem. Anal. Des., vol. 187, pp. 103510, 2021. Doi: 10.1016/j.finel.2020.103510.

A. Kalhor, M. Soleimani, H. Mirzadeh, and V. Uthaisangsuk, “A review of recent progress in mechanical and corrosion properties of dual phase steels,” Arch. Civ. Mech. Eng., vol. 20, no. 3, pp. 1-14, 2020. Doi: 10.1007/s43452-020-00088-0.

A. Kalhor and H. Mirzadeh, “Tailoring the microstructure and mechanical properties of dual phase steel based on the initial microstructure,” Steel Res. Int., vol. 88, no. 8, pp. 1-8, 2017. Doi: 10.1002/srin.201600385.

F. Jamei, H. Mirzadeh, and M. Zamani, “Synergistic effects of holding time at intercritical annealing temperature and initial microstructure on the mechanical properties of dual phase steel,” Mater. Sci. Eng. A, vol. 750, pp. 125-131, 2019. Doi: 10.1016/j.msea.2019.02.052.

J. Adamczyk, and A.Grjcar "Heat treatment and mechanical properties of low-carbon steel with dual-phase microstructure

," Journal of Achievement in Materials and Manufacturing Engineering, vol. 22, no. 1, 2007.

H. Dannoshita, T. Ogawa, K. Maruoka, and K. Ushioda, “Effect of initial microstructures on austenite formation behavior during intercritical annealing in low-carbon steel,” Mater. Trans., vol. 60, no. 1, pp. 165-168, 2019. Doi: 10.2320/matertrans.M2018298.

M. Maleki, H. Mirzadeh, and M. Zamani, “Effect of intercritical annealing time at pearlite dissolution finish temperature (Ac1f) on mechanical properties of low-carbon dual-phase steel,” J. Mater. Eng. Perform., vol. 28, no. 4, pp. 2178-2183, 2019. Doi: 10.1007/s11665-019-04009-y.

M. Maleki, H. Mirzadeh, and M. Zamani, “Effect of intercritical annealing on mechanical properties and work-hardening response of high formability dual phase steel,” Steel Res. Int., vol. 89, no. 4, pp. 1-7, 2018. Doi: 10.1002/srin.201700412.

ASTM International, “Standard test methods for determining average grain size,” E 112-12, 2010. Doi: 10.1520/E0112-12.1.4.

J. Adamczyk and A. Grajcar, “Heat treatment and mechanical properties of low-carbon steel with dual-phase microstructure manufacturing and processing,” J. Achiev. Mater. Manuf. Eng., vol. 22, no. 1, pp. 13-20, 2007.

N. Lanzillotto and F. B. Pickering, “Structure-property dual-phase steels relationships in,” Met. Sci., vol. 16, no. August, pp. 371-382, 1982.

M. A. M. Gurgel, E. S. B. Junior, R. S. Teixeira, G. O. Nascimento, S. S. Oliveira, D. N. F. Leite, L. P. Moreira, L. P. Brandao, and A. S. Paula , “Microstructure and continuous cooling transformation of an Fe-7.1Al-0.7Mn-0.4C-0.3Nb Alloy,” Metals (Basel)., vol. 12, no. 8, pp. 1-16, 2022. Doi: 10.3390/met12081305.

P. D. Basoeki, “Effects of DP steel microstructure on the disappearance of discontinuous yielding,” MATEC Web Conf., vol. 204, pp. 1-8, 2018. Doi: 10.1051/matecconf/201820407013.

Y. G. Deng, H. S. Di, and R. D. K. Misra, “On significance of initial microstructure in governing mechanical behavior and fracture of dual-phase steels,” J. Iron Steel Res. Int., vol. 25, no. 9, pp. 932-942, 2018. Doi: 10.1007/s42243-018-0133-0.

H. Mirzadeh, M. Alibeyki, and M. Najafi, “Unraveling the initial microstructure effects on mechanical properties and work-hardening capacity of dual-phase steel,” Metall. Mater. Trans. A Phys. Metall. Mater. Sci., vol. 48, no. 10, pp. 4565-4573, 2017. Doi: 10.1007/s11661-017-4246-z.

Y. Mazaheri, A. Kermanpur, and A. Najafizadeh, “A novel route for development of ultrahigh strength dual phase steels,” Mater. Sci. Eng. A, vol. 619, pp. 1-11, 2014. Doi: 10.1016/j.msea.2014.09.058.

Z. Zhao, T. Tong, J. Liang, H. Yin, A. Zhao, and D. Tang, “Microstructure, mechanical properties and fracture behavior of ultra-high strength dual-phase steel,” Mater. Sci. Eng. A, vol. 618, pp. 182-188, 2014. Doi: 10.1016/j.msea.2014.09.005.

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