Sintesis dan Karakterisasi Material Nano-Perovskite Neodymium Iron Oxide (NdFeO3)

Rina Dewi Mayasari

Abstract

Sintesis nano-perovskite neodymium iron oxide (NdFeO3) telah berhasil dilakukan dengan metode presipitasi menggunakan surfaktan ethylene glycol (EG) sebagai coating material. Senyawa NdFeO3 dikarakterisasi analisis gugus fungsi kimia dengan Fourier transform infrared spectroscopy (FTIR), analisis morfologi dengan scanning electron microscopy (SEM), analisis kristalinitas dan ukuran partikel dengan X-ray diffraction (XRD) dan transmission electron microscopy (TEM). Pengamatan SEM dan TEM menunjukkan bahwa hasil sintesis membentuk nanostruktur berbentuk bulat dengan ukuran diameter pada rentang 15 sampai 20 nm. Spektra XRD mengonfirmasi bahwa fasa NdFeO3 membentuk struktur orthorombik dan perovskite.

Keywords

nano-perovskite; NdFeO3; ethylene glycol; presipitasi

Full Text:

PDF

References

J. Shanker, G.N. Rao, K. Venkataramana, and D.S. Babu, “Investigation of structural and electrical properties of NdFeO3 perovskite nanocrystalline,” Phys. Lett. A, vol. 382, pp. 2974-2977, Oct. 2018.

T.A. Nguyen, M.V. Berezhnaya, T.L. Pham, V.O. Mittova, M.Q. Vo, L.T.Tr. Nguyen, H. Tr. Do, I.Ya. Mittova, and E.L. Viryutina, “Synthesis and magnetic characteristics of neodymium ferrite powders with perovskite structures”, Russ. J. Appl. Chem., vol. 92, no. 4, pp. 458-464, 2019.

M. Nakhei and D.S. Khoshnoud, “Influence of particle size and lattice distortion on magnetic and dielectric properties of NdFeO3 orthoferrite”, Physica B-Cond. Matt., vol. 553, pp. 53-58, Oct. 2019.

Y. Chen, D. Wang, H. Qin, H. Zhang, Z. Zang, G. Zhou, C. Gao, and J. Hu, “CO2 sensing properties and mechanism of PrFeO3 and NdFeO3¬ thick tilm sensor”, J. Rare Earths, vol. 37, issue 1, pp. 80-87, Jan. 2019.

M.K. Motlagh, M. Noroozifar, M. Yousefi, and Sh. Jahani, “Chemical synthesis and characterization of perovskite NdFeO3 nanocrystal via a co-precipitation method”, International Journal of Nanotechnology. Vol. 9, No. 1, pp. 7-14, 2013.

E.H. Sujiono, M.Y. Dahlan, R.A. Imran, A.C.M. Said, and S. Samnur, “The effects of calcination temperatures on crystal structures and morphologies of Nd1.2FeO3 synthesized by solid-state reaction”, in IOP Conf. Ser.: Mater. Sci. Eng., vol. 367, p. 012042, 2018.

N.F. Atta, A. Galal, and E.H. El-Alds, “Perovskite nanomaterials-synthesis, characterization, and applications”, in Perovskite materials: synthesis, characterisation, properties, and applications. [Online], Available: https://www.intechopen.com/

Z. Anajafi, M. Naseri, S. Marini, C. Espro, D. Lannazzo, S.G. Leonardi, and G. Neri, “NdFeO3 as a new electrocatalytic material for the electrochemical monitoring of dopamine”, Anal. Bioanal. Chem., Jul. 2019.

M. Yousefi, S.S. Zeid, and M.K. Motlagh, “Synthesis and characterization of nano-structured perovskite type neodymium orthoferrite NdFeO3”, Curr. Chem. Lett., vol. 6, pp. 23-30, 2017.

J. Shanker, M.B. Suresh, and D.S. Babu, “Synthesis, Characterization and Electrical Properties of NdXO3 (X=Cr, Fe) Nanoparticles, Mat. Today.: Proc., vol. 3, pp. 2091-2100, 2016.

C.M. Hussain, “Magnetic Nanomaterials for Environmental Analysis”, in Advanced environmental analysis: applications of nanomaterials, vol. 2, B. Kharisov, Cambridge: Royal Society of Chemistry, 2017, pp. 3-13.

Copyright (c) 2020 Metalurgi
Creative Commons License
This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.

Refbacks

  • There are currently no refbacks.